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Microcalorimetric investigation of water vapor adsorption on silica gel
Microcalorimetry Diffusivity Silica gel–water pair Heat of adsorption
2011/11/10
Water vapor adsorption on silica gel was investigated using Tian–Calvet-type microcalorimetry. Differential heat of adsorption data was obtained. The setup of microcalorimetry was used volumetric syst...
Friedel-Crafts acylation of arenes with carboxylic acids using silica gel supported AlCl3
Acylation aluminium trichloride ketones silica gel
2010/10/19
Aromatic compounds react smoothly with carboxylic acids in the presence of silica gel supported aluminium trichloride to afford the corresponding ketones with high regioselectivity in high to excellen...
Simultaneous Determinations of Cr(VI) and Cr(III) by Ion-Exclusion/Cation-Exchange Chromatography with an Unmodified Silica-Gel Column
Cr(VI) Cr(III) Ion-Exclusion/Cation-Exchange Chromatography an Unmodified Silica-Gel Column
2010/9/19
In order to characterize the ion-exclusion and cation-exchange properties of an unmodified silica-gel column, the retention behaviors of Cr(VI) and Cr(III) ions were investigated using a Develosil 30-...
Solid-Phase Extractors Based on 8-Aminoquinoline and 2-Aminopyridine Covalently Bonded to Silica Gel for the Selective Separation and Determination of Calcium in Natural Water and Pharmaceutical Samples
Solid-Phase Extractors 8-Aminoquinoline 2-Aminopyridine Covalently Bonded Silica Gel the Selective Separation Calcium
2010/9/20
Two new silica-gel phases were produced directly via the chemical interaction of 3-chloropropyltrimethoxysilane modified silica gel with 8-aminoquioline, phase I and 2-aminopyridine, phase II under re...
酞菁键合硅胶的制备及分离取代酞菁异构体（Preparation of Phthalocyanine Bonded Silica Gel for the Separation of Phthalocyanine Isomers）
酞菁键合硅胶 制备 分离 异构体
2010/8/18
制备和表征了一种新的酞菁键合硅胶，三-β-(辛巯基)-β-(磺酰胺基)-酞菁铜键合硅胶。研究了该键合酞菁硅胶作为HPLC固定相的基本色谱性能。实验结果表明，该固定相可以分离四-α-(2，2，4-三甲基-3-戊氧基)酞菁(铜、镍)的4种异构体，也可以观察到四-α-(2，2，4-三甲基-3-戊氧基)无金属酞菁的4种异构体，而商业C18(VERTEX Eurospher)却只能观察到两组峰，表明这种酞菁...
Formation of the Monolithic Silica Gel Column with Bimodal Pore Structure
Monolithic silica gel column Phase separation Sol-gel transition Pore structure
2010/4/20
A biporous monolithic silica gel column possessing both micrometer sized through-pores and nanometer sized mesopores located in the silica skeletons was prepared and the high concentration porogen (e....
Effects of Acidity on the Hydrothermal Synthesis of Kaolinite from Silica-Gel and Gibbsite
Crystallite size Crystallization Hydrothermal synthesis Kaolinite pH Stacking fault
2011/12/27
Abstract: A comparative study is reported in which kaolinite has been hydrothermally synthesized at several pH conditions. The syntheses were carried out at 220 亱C for 3 to 10 d with distilled water o...
Apparent and Partial Specific Sorption of Oxine by Montmorillonite and Silica Gel in Binary Mixtures
Adsorption Mixtures Montmorillonite Oxine Silica gel Specific sorption
2012/1/12
Oxine sorption by binary mixtures of montmorillonite and silica gel was studied at pH 5 as a function of oxine concentration and mixture composition. The investigation was made to resolve the problem ...